Equipment
Equipment
Within the laboratory we have the ability to synthesise catalysts by a variety of standard methods. In terms of catalyst characterisation, we are well equipped in-house:
- Routine volumetric physisorption analysis (i.e., surface area, pore size, pore volume)
- Chemisorption methods (both volumetric and dynamic)
- Temperature programmed methods (i.e., TPR, TPD & TPO)
- FTIR analysis using probe molecules (CO for metals & pyridine for acid sites)
Catalyst testing can be performed in either batch or flow reactors:
- Autoclave reactors for batch reactions at elevated pressures
- Atmospheric or pressurised systems for gas phase flow reactors
- Pressurised systems for 3-phase continuous flow studies
- In-situ/operando reaction experiments using combined FTIR and Mass Spectrometry
We also make use of central facilities (TGA, XRD, SEM & EDX) and collaborate for access to other specialised techniques (TEM and XPS)